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Avishek Chanda | Nam Kyeun Kim | Debes Bhattacharyya, May 2021
In the current research, hybrid laminates having veneer facesheets and natural fibre composite cores were fabricated to investigate their fire and mechanical properties and to observe a suitable combination. Wool and flax fibres were selected for fibre reinforcement. Ammonium polyphosphate (APP) was used as the primary flame retardant for all the composites. The mechanical performance of the flax fibre reinforced fire retardant polypropylene (flax-FRPP) and fire retardant wool-polypropylene (FR-wool-PP) hybrid layered panels were further studied and compared to plywood made similarly. The results showed that hybrid laminates have better fire properties and the hybrid layered veneer composites can have significant structural applications if proper bonding between the composite and the veneer layers can be achieved. The tensile properties showed a reduction in Young’s modulus and ultimate tensile strength, though the wool-veneer hybrid laminates outperformed the flax-veneer ones. Moreover, the impact test showed that the wool-veneer hybrid laminates had the best resistance when compared to all the veneer-based samples tested. The results point towards the possibility of manufacturing a superior fire-resistant hybrid veneer composite laminate.
Mai T. K. Dang | Mostafa Nikzad | Khanh V. Truong | Syed Masood | Igor Sbarski, May 2021
The present study aims to design a comonomer based resin matrix with a prolonged gel time while maintaining low viscosity and minimal curing time to ensure its processability with high filler contents in fabricating polymer concrete composites (PCC) for bases of tool machines. In this work, a copolymerization route was adopted to optimize the processability of a commercially available epoxy vinyl ester. Comonomer resin systems were prepared from addition of Methyl methacrylate (MMA) as a reactive diluent into the commercial epoxy vinyl ester resin (VE) which was premixed with styrene (ST) diluent (48 wt. %). Compositions of comonomer resin systems were varied systematically to achieve an optimum mixture design. The viscosity and gel time of comonomer resin systems were measured by a digital Brookfield viscometer. The influence of MMA on the curing behavior, elastic modulus and glass transition temperatures of comonomer resin systems have been investigated by differential scanning calorimeter (DSC) and dynamic mechanical analyses (DMA) respectively. The obtained optimum comonomer resin system was 40wt% VE resin, 23wt% MMA and 37wt% ST. This formulation exhibited 80% lower viscosity and about 45% longer gel time as compared to the viscosity and gel time of commercial VE resin system with just half the styrene monomer content, thereby not only ensuring its processing with high filler contents, but also reducing the volatile organic compounds associated with the large-scale manufacturing of PCC products. Also, this composition showed the shortest curing time and 60% higher flexural strength (53.6 MPa) compared to that of the commercial VE resin system (17.3MPa).
Hima Haridevan | David Birnie | David A.C. Evans | Darren J. Martin | Pratheep K. Annamalai, May 2021
The incorporation of technical lignin, a multifunctional natural polymer, into rigid polyurethane foam (RPUF) for the enhancement of thermal insulation performance has gained increasing interest in academia and industry. However, the structural complexity of technical lignin hinders its dispersion in the polyols commonly used for the preparation of RPUF.
Poor dispersion of technical lignin in polyols inhibits the chemical reactions and limits the potential improvement in the thermal and mechanical properties of RPUF. Herein we report enhanced dispersion of unmodified kraft lignin, at a loading of 3 wt % in a mixture of glycerol and an aromatic polyester polyol (20:80) for the preparation of RPUF. It has improved the insulation property by 30% while retaining its mechanical performance compared to the control RPUF without lignin.
Such a level of improvement, to the best of our knowledge, has not been reported in RPUF using chemically unmodified lignin to date. This is attributed to the enhanced dispersion of the kraft lignin in the polyol blend causing changes in the cell morphology of the resultant RPUF, as supported by microscopic and rheological analysis. To this end, the insights into the influence of kraft lignin on the polyol-precursor on the properties of the RPUF are discussed.
J.N. Saucedo-Zuñiga | S. Sánchez-Valdes | E. Ramírez-Vargas | L. Guillen | L. F. Ramos-deValle | J.A. Rodriguez, May 2021
The preparation and characterization of a multilayer film reservoir with clay/essential oil (EO) composites was described. The goal is to analyze the potential use of these reservoirs with clay/EOs composites as aroma-controlled release for various applications such as pesticide or attractant for pest control as well as antimicrobial control. Two types of clays were analyzed, porous halloysite (HNT) and octadecyl modified montmorillonite (MMT) nanoclay; as well as two types of essential oils, orange (OO) and thyme oil (TO). The DRX results confirmed that MMT clay presented higher thyme oil adsorption and better interactions than orange oil. Clay/EO composites encapsulated in multilayer film showed a prolongated aroma release during longer times. Polyamide (PA) barrier layer thickness has an effect on the liberation of the volatile compounds through the multilayer film.
Valentina A. Woodcraft | Ellen C. Keene | Phillip Lin | Gerald K. LeBlanc, May 2021
ASTM D-2863 is a small-scale fire performance classification test, part of ASTM C-578 standard for polystyrene rigid thermal insulations, with a binary pass/fail outcome at a given oxygen concentration level. When applied to foams, the test is highly variable and is easy to manipulate, putting its accuracy as a test method into question. In this work, macro-imaging was used to closely monitor the foam – flame interaction to gain a better understanding of variability levers. For example, one of the levers is duration of flame application to a sample. Our imaging studies indicate that the pass / fail boundary oxygen level is strongly correlated with the flame application duration.
Liqing Wei | Ruomiao Wang | Mark O. Mason, May 2021
In this paper, a decorative material was first applied onto the light weight reinforced thermoplastic (LWRT) composite core mat during the core manufacturing, and then followed by a consolidation process through the calender rolls. This method is defined as an in-line lamination process with a finished A-surface panel in comparison with conventional off-line decorative materials lamination process, in which the decorative layer is applied in a separate process from core manufacture. Decorative layers with two patterns, namely woodgrain and marble, have been studied. The adhesion performance between the decorative skin material and LWRT composite substrate has been evaluated by 180° peel adhesion test following ASTM standard D903. The separation between the decorative layer and the substrate was difficult to initiate, which demonstrates an outstanding adhesion between the two components. A stylus method quantitatively confirmed the decorative surface is smooth and able to cover the core’s texture. Flatwise tensile test results by ASTM standard C297 method showed the decorative panels could not be delaminated, indicating strong bonding between decorative skin material and core mat. Materials produced with the woodgrain pattern were tested to have better flexural strength and stiffness than the sample made with marble decorative pattern material. In addition, flame retardancy results showed the laminated decorative panels can meet ASTM E84 requirement of Class C and above. The decorative material with custom design provides the decorative A-surface with an appearance of wood, stone, textile or other natural materials as desired, opening a window for the LWRT composite to be used inside an RV such as the interior layer of sidewall and ceiling.
Kim McLoughlin Senior Research Engineer, Global Materials Science Braskem
A Resin Supplier’s Perspective on Partnerships for the Circular Economy
About the Speaker
Kim drives technology programs at Braskem to develop advanced polyolefins with improved recyclability and sustainability. As Principal Investigator on a REMADE-funded collaboration, Kim leads a diverse industry-academic team that is developing a process to recycle elastomers as secondary feedstock. Kim has a PhD in Chemical Engineering from Cornell. She is an inventor on more than 25 patents and applications for novel polyolefin technologies. Kim is on the Board of Directors of SPE’s Thermoplastic Materials & Foams Division, where she has served as Education Chair and Councilor.
A Resin Supplier’s Perspective on Partnerships for the Circular Economy
About the Speaker
Gamini has a BS and PhD from Purdue University in Materials Engineering and Sustainability. He joined Penn State as a Post Doctorate Scholar in 2020 prior to his professorship appointment. He works closely with PA plastics manufacturers to implement sustainability programs in their plants.
A Resin Supplier’s Perspective on Partnerships for the Circular Economy
About the Speaker
Tom Giovannetti holds a Degree in Mechanical Engineering from The University of Tulsa and for the last 26 years has worked for Chevron Phillips Chemical Company. Tom started his plastics career by designing various injection molded products for the chemical industry including explosion proof plugs and receptacles, panel boards and detonation arrestors for 24 inch pipelines. Tom also holds a patent for design of a polyphenylene sulfide sleeve in a nylon coolant cross-over of an air intake manifold and is a Certified Plastic Technologist through the Society of Plastic Engineers. Tom serves on the Oklahoma Section Board as Councilor, is also the past president of the local Oklahoma SPE Section, and as well serves on the SPE Injection Molding Division board.
Joseph Lawrence, Ph.D. Senior Director and Research Professor University of Toledo
A Resin Supplier’s Perspective on Partnerships for the Circular Economy
About the Speaker
Dr. Joseph Lawrence is a Research Professor and Senior Director of the Polymer Institute and the Center for Materials and Sensor Characterization at the University of Toledo. He is a Chemical Engineer by training and after working in the process industry, he has been engaged in polymers and composites research for 18+ years. In the Polymer Institute he leads research on renewably sourced polymers, plastics recycling, and additive manufacturing. He is also the lead investigator of the Polyesters and Barrier Materials Research Consortium funded by industry. Dr. Lawrence has advised 20 graduate students, mentored 8 staff scientists and several undergraduate students. He is a peer reviewer in several journals, has authored 30+ peer-reviewed publications and serves on the board of the Injection Molding Division of SPE.
Matt Hammernik Northeast Account Manager Hasco America
A Resin Supplier’s Perspective on Partnerships for the Circular Economy
About the Speaker
Matt Hammernik serves as Hasco America’s Northeast Area Account Manager covering the states Michigan, Ohio, Indiana, and Kentucky. He started with Hasco America at the beginning of March 2022. Matt started in the Injection Mold Industry roughly 10 years ago as an estimator quoting injection mold base steel, components and machining. He advanced into outside sales and has been serving molders, mold builders and mold makers for about 7 years.
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Any article that is cited in another manuscript or other work is required to use the correct reference style. Below is an example of the reference style for SPE articles:
Brown, H. L. and Jones, D. H. 2016, May.
"Insert title of paper here in quotes,"
ANTEC 2016 - Indianapolis, Indiana, USA May 23-25, 2016. [On-line].
Society of Plastics Engineers, ISBN: 123-0-1234567-8-9, pp. 000-000.
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Note: if there are more than three authors you may use the first author's name and et al. EG Brown, H. L. et al.